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Paper | Regular issue | Vol 43, No. 12, 1996, pp. 2747 - 2755
Published online:
DOI: 10.3987/COM-96-7641
Structure Elucidation and Synthesis of a Metabolite of Antiinflammatory Drug DUP 697

Shizuo Nakamura, Mitsuyoshi Kondo, Kiyoto Goto, Mitsuhiro Nakamura, Yoshiaki Tsuda, and Kozo Shishido*

*Institute for Medicinal Resources, University of Tokushima, Sho-machi, Tokushima 770-8505, Japan

Abstract

Structure of the O-glucuronide (2), one of the metabolites of antiinflammatory drug DUP 697 (1), has been elucidated on the basis of spectral data and a total synthesis of it has been accomplished. Since the synthetic route to 2 is an unambiguous one, complection of the synthesis established the assigned sturcture.

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