HETEROCYCLES
An International Journal for Reviews and Communications in Heterocyclic ChemistryWeb Edition ISSN: 1881-0942
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Obituary
Yoshito Kishi (1937-2023)
Yoshito Kishi (1937-2023)
Professor. Yoshito Kishi,
a member of the Honorary Editorial Associates of HETEROCYCLES,
has passed away on January 9, 2023 at the age of 85.
I deeply express my regret over his death.
Kunio Ogasawara
Editor
January 13, 2023
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December 24, 2019
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e-Journal
Abstract
1 data found. 1 - 1 listed
Communication | Special issue | Vol 103, No. 1, 2021, pp. 205 - 217
Published online: 19th October, 2020
Supporting Info. (1.9MB)PDF (772KB)PDF with Links (1.4MB)
Published online: 19th October, 2020
DOI: 10.3987/COM-20-S(K)24
■ Rhodium-Catalyzed Crossed [2+2+2] Cycloaddition with Ynamides: Key-Strategy for the Concise Total Synthesis of 3-Oxygenated Carbazole Alkaloids
Carole Alayrac* and Bernhard Witulski*
*Laboratoire de Chimie Molèculaire et Thioorganique (LCMT) , National Graduate School of Engineering and Research Center, France
Abstract
Total syntheses of a set of naturally occurring 3-oxygenated carbazole alkaloids - 6-chlorohyellazole, carazostatin, carbazomycins A and B - are described. The key-strategy underlines a highly chemo- and regioselective rhodium-catalyzed [2+2+2] cyclotrimerization between appropriately tailored yne-ynamides and 1-methoxypropyne that is stirred by the interplay of stereoelectronic and steric effects allowing the introduction of four ring substituents of the natural carbazoles within a single step and making the overall syntheses short and efficient.
1 data found. 1 - 1 listed
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