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Paper | Regular issue | Vol 57, No. 6, 2002, pp.1017-1032
Published online, 1st January, 1970■ Synthesis of 3-Substituted 5-Arylidene-1-methyl-2-thiohydantoins under Microwave Irradiation
Published online, 1st January, 1970
DOI: 10.3987/COM-02-9452
■ Synthesis of 3-Substituted 5-Arylidene-1-methyl-2-thiohydantoins under Microwave Irradiation
Ahmed I. Khodair and John Nielsen*
*Department of Chemistry, Technical University of Denmark, Kemitorvet, Building 207, DK-2800 Kgs. Lyngby, Denmark
Abstract
A mono-modal microwave oven was used to expedite the synthesis of small libraries of 3-substituted 1-methyl-2-thiohydantoins and 3-substituted 5-arylidene-1-methyl-2-thiohydantoins. In comparison with the traditional reflux methods, similar or higher yields were obtained.
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