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Paper | Special issue | Vol 76, No. 1, 2008, pp.291-303
Published online, 29th February, 2008
DOI: 10.3987/COM-08-S(N)8
Synthesis of Highly Oxygenated Biphenyl Derivative in an Optically Active Form through Palladium-Mediated Intramolecular Biaryl Coupling Reaction

Hitoshi Abe,* Masatsugu Arai, Keisuke Nishioka, Tatsuya Kida, Kazuma Shioe, Yasuo Takeuchi, and Takashi Harayama*

*Advanced Science Research Center, Okayama University, Okayama 700-8530, Japan

Abstract

Optically active 6,6’-dihydroxymethyl-2,2’-3,3’-4,4’-hexamethoxybiphenyl (1) was prepared via the Pd-mediated biaryl coupling reaction of a phenyl benzoate derivative and the following enantioselective lactone opening reaction.