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Paper | Regular issue | Vol 32, No. 11, 1991, pp.2225-2240
Published online, 1st January, 1970
DOI: 10.3987/COM-91-5872
Synthesis of D-Allosan from Levoglucosenone

Katsuya Matsumoto,* Takashi Ebata,* Koshi Koseki, Hiroshi Kawakami, and Hajime Matsushita

*Life Science Research Laboratory, Japan Tobacco Inc., 6-2, Umegaoka, Midori-ku, Yokohama, Kanagawa 227-8512, Japan

Abstract

The stereoselective reduction and cis-dihydroxylation of levoglucosenone (1,6-anhydro-3,4-dideoxy-β-D-glycero-hex-3-enopyranos-2-ulose), gave D-allosan (1,6-anhydro-β-D-allopyranose) in high yield.