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Obituary
Zenichi Yoshida (1925-2023)
Zenichi Yoshida (1925-2023)
Professor. Zenichi Yoshida,
a member of the Honorary Advisors of HETEROCYCLES (1975-1998),
has passed away on May 4, 2023 at the age of 97.
I deeply express my regret over his death.
Kunio Ogasawara
Editor
May 11, 2023
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Paper | Regular issue | Vol 48, No. 1, 1998, pp.41-51
Published online, 1st January, 1970■ The Reaction of Unsaturated Carbonyl Compounds with "Activated" Sulfur (II). Formation of Cyclic Disulfide and Polysulfides
Published online, 1st January, 1970
DOI: 10.3987/COM-97-7967
■ The Reaction of Unsaturated Carbonyl Compounds with "Activated" Sulfur (II). Formation of Cyclic Disulfide and Polysulfides
Ugo Chiacchio, Antonino Corsaro, Venerando Pistarà, Giovanni Purrello,* and Antonio Rescifina
*Dipartimento di Scienze Chimiche, Università di Catania, Viale A. Doria 6, I-95125 Catania, Italy
Abstract
From the reaction of cinnamylideneacetophenone (1), sulfur and triethylamine in suitable solvents at room temperature, phenyl{3-[(E)-1-((5-benzoyl-3H-1,2-dithiol-3-ylidene)phenylmethyldisulfanyl)-1-phenylmethylidene]-3H-1,2-dithiol-5-yl}methanone (7) was isolated together with two polysulfurated compounds to which structures of phenyl(7-phenyl-1,2,3-trithiepin-4-yl)methanone (12) and phenyl(8-phenyl-1,2,3,4-tetrathiocin-5-yl)methanone (13) were assigned. The obtaining of these new products allows to complete the sequence of the whole process.
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