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Note | Regular issue | Vol 48, No. 4, 1998, pp.749-754
Published online, 1st January, 1970
DOI: 10.3987/COM-97-8077
Electrochemical Synthesis of 2,1-Benzisoxazoles by Controlled Potential Cathodic Electrolysis

Byeong Hyo Kim,* Young Moo Jun, Yong Rack Choi, Doo Byung Lee, and Woonphil Baik

*Department of Chemistry, Kwangwoon University, 447-1, Wolgye-Dong Nowon-ku, Seoul, 139-701, Korea

Abstract

Using a divided cell, reductive cyclization of nitroarene compounds into 2,1-benzisoxazoles in mild conditions was successfully accomplished by the controlled potential cathodic electrolysis reactions. Optimum reaction potential of each reaction was determined based on cyclic voltametric behavior in methanol solution at Pb or Pt cathode, and Pt anode.