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Communication | Special issue | Vol 52, No. 1, 2000, pp.73-79
Published online, 1st January, 1970■ Thermal Ring Transformation of 2,2-Disubstituted Benzothiazoline 1-Oxides
Published online, 1st January, 1970
DOI: 10.3987/COM-99-S11
■ Thermal Ring Transformation of 2,2-Disubstituted Benzothiazoline 1-Oxides
Hiroshi Shimizu,* Michiko Kanematsu, Kiyomi Hashimoto, and Kazuhiro Kobayashi
*Gifu Pharmaceutical University, 6-1 Mitahora-higashi 5-chome, Gifu 502-8585, Japan
Abstract
Thermal rearrangement of 2,2-disubstituted benzothiazoline 1-oxides (1) in aprotic solvent afforded the corresponding 1,4-benzothiazines (2) and (3). The thermal reaction performed in the presence of electron-deficient acetylenic compounds produced new tricyclic compounds (7) whose structures have been established by an X-Ray crystal structure determination.
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