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Report | Regular issue | Vol 19, No. 11, 1982, pp.2131-2138
Published online, 1st January, 1970
DOI: 10.3987/R-1982-11-2131
New 1,10-Phenanthrolinethioles

Max Hunziker and Urs Hauser

*Department of Physics, Stanford University, Stanford, CA 94305, U.S.A.

Abstract

Reaction of KHS with 2-chloro- and 2,9-dichloro-1,10-phenanthroline in ethanol at elevated temperature and pressure afforded the corresponding phenanthrolinethiols which were characterized by spectroscopic and chemical methods. 2,2’-Thiobis(1,10-phenanthroline) and other heteroaryl sulfides derived from 1,10-phenanthroline-2-thiol were prepared by amide promoted nucleophilic substitution of aryl halide by thiolate anion.