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Communication | Regular issue | Vol 22, No. 3, 1984, pp.485-488
Published online, 1st January, 1970
DOI: 10.3987/R-1984-03-0485
New Synthetic Route to Perhydrohistorionicotoxin Using (3Z)-4-Butyl-3-trichloroacetamido-1,3-butadiene

Toshiro Ibuka,* Hiroyuki Minakata, Masaya Hashimoto, Larry E. Overman, and Robert L. Freeks

*Department of Chemistry, University of California, Irvine, Irvine, California 92697, U.S.A.

Abstract

A formal synthesis of perhydrohistrionicotoxin via the Diels-Alder cycloadduct obtained by reaction of (3Z)-4-butyl-3-trichloroacetamido-1,3-butadiene with methyl acrylate is presented.