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Report | Regular issue | Vol 24, No. 6, 1986, pp.1599-1603
Published online, 1st January, 1970
DOI: 10.3987/R-1986-06-1599
Synthesis and Structure of 6-Phenylcyclophosphamides

Yun-Er Shih,* Jy-shih Wang, and Ling-Kang Liu

*Institutue of Chemistry, Academia Sinica, 128, Yan-Chiu-Yuan Road, Sec II, Nankang, Taipei,11529, Taiwan, R.O.C.

Abstract

6-Phenylcyclophosphamides have been synthesized from methyl benzoate and acetonitrile to benzoyl acetonitrile followed by reduction to amino alcohol and condensation with bis(2-chloroethyl)phosphoramidic dichloride. The two diastereomers have been separated and their structures have been assigned on the basis of ir, P-31 nmr and X-ray crystallography.