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Communication | Regular issue | Vol 24, No. 7, 1986, pp.1831-1834
Published online, 1st January, 1970
DOI: 10.3987/R-1986-07-1831
The Reaction of 1-Alkoxycarbonyl-1H-azepine with Palladium Acetane in Benzene

Katsuhiro Saito*

*Faculty of Engineering, Nagoya Institute of Technology, Gokiso-cho, Showa-ku, Nagoya 466-8555, Japan

Abstract

Heating of 1-alkoxycarbonyl-1H-azepines in benzene in the presence of palladium acetate followed by addition of water afforded 2-alkoxycarbonyl-7-phenyl-2-azabicyclo[4.1.0]hept-4-en-3-ols via reaction of the azepines with palladium salt coordinated by phenyl group, which is derived from palladium acetate and benzene.