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Short Paper | Special issue | Vol 84, No. 2, 2012, pp.1285-1288
Published online, 21st July, 2011
DOI: 10.3987/COM-11-S(P)40
Reinvestigation of the Classical Total Synthesis of Makomakine

Makoto Furuya, Ayumi Nagatomo, and Masahiro Toyota*

*Department of Chemistry, Graduate School of Science, Osaka Prefecture University, 1-1 Gakuencho, Sakai, Osaka 593-8531, Japan


Reinvestigation of the original Stevens synthesis of makomakine showed that the yield of the Ritter reaction of 3-indoylacetonitrile with (–)-β-pinene could be increased by employing Hg(OTf)2.