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Short Paper | Regular issue | Vol 87, No. 1, 2013, pp.147-154
Published online, 15th November, 2012
DOI: 10.3987/COM-12-12601
A New Synthesis of Amino Substituted Azolo[1,3,5]triazines via Reaction of N1,N1-Dimethyl-N2-azolylformamidines with Cyanamide

Dmitrii V. Kalinin, Svetlana A. Kalinina, and Anton V. Dolzhenko*

*School of Pharmacy, Curtin University of Technology, GPO Box U1987, Perth, Western Australia 6845, Australia

Abstract

The amino substituted triazine ring was annelated to aminoazoles using a new effective synthetic procedure. The method of preparation involved initial formation of azolylformamidines in the reaction of aminoazoles with N,N-dimethylformamide dimethyl acetal followed by the triazine ring closure with cyanamide affording therefore fused aminotriazines.