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Communication | Special issue | Vol 88, No. 1, 2014, pp.207-212
Published online, 1st August, 2013
DOI: 10.3987/COM-13-S(S)72
Preparation and Electrochemical Property of Octaethylphthalocyanine Fused with Four Diselenadithiafulvalene Units

Takeshi Kimura*

*Center for Instrumental Analysis, Iwate University, 4-3-5 Ueda, Morioka, Iwate 020-8551, Japan

Abstract

3,6-Diethylphthalonitrile (3) fused with diselenadithiafulvalene (DSDTF) was prepared from 5,6-dibromo-4,7-diethylbenzotriselenole (1) and treated with lithium alkoxide to produce octaethylphthalocyanine (6) with four DSDTF units. The structure of the product was determined by 1H NMR and MALDI-TOF-MS. Electrochemical and optical properties of 6 and its nickel complex (6-Ni) were examined by cyclic voltammetry and UV-vis spectroscopy.