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Short Paper | Regular issue | Vol 87, No. 9, 2013, pp.1917-1924
Published online, 31st July, 2013
DOI: 10.3987/COM-13-12771
ONE-POT SYNTHESIS OF 11,23-BIS(IMIDAZOL-1-YL)CALIX[4]ARENE DERIVATIVES BASED ON THE UPPER RIM OF BIS-AMINOCALIX[4]ARENE

Bing Zhao, Yao-Yu Ruan, Ming-jie Ma, Qi-Gang Deng,* Li-Yan Wang, Ya-Qing Feng, and Yan Gao*

*College of Chemistry and Chemical Engineering, Qiqihar University, 42 Wenhuadajie, Qiqihar, Heilongjian Shang, 161006, China

Abstract

A simple one-pot synthesis for a new 11,23-bis(imidazol-1-yl)calix[4]arene derivatives in their cone conformation was reported by the four component condensation reaction of 11,23-bis-aminocalix[4]arene, aldehyde, benzil and ammonium acetate. This work provides a simple, efficient method for the construction of 11,23-bis(imidazol-1-yl)calix[4]arene derivatives on which the substituted imidazole rings are directly linked to their upper rim.