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Obituary
Zenichi Yoshida (1925-2023)
Zenichi Yoshida (1925-2023)
Professor. Zenichi Yoshida,
a member of the Honorary Advisors of HETEROCYCLES (1975-1998),
has passed away on May 4, 2023 at the age of 97.
I deeply express my regret over his death.
Kunio Ogasawara
Editor
May 11, 2023
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Paper | Regular issue | Vol 87, No. 10, 2013, pp.2023-2029
Published online, 10th September, 2013
Published online, 10th September, 2013
DOI: 10.3987/COM-13-12789
■ Facile Synthesis of Indolines by a Tandem Nitro-reduction Aza Michael Addition Reaction
Wellington Martins Ventura, Luiz Guilherme Souza de Assis, and Jason Guy Taylor*
*Department of Chemistry, Federal University of Ouro Preto, Bauxita, ICEB, UFOP, Ouro Preto 35400-000, Brazil
Abstract
A diverse array of substrates are conveniently prepared by coupling diazonium salts to ethyl vinyl ether and subjecting the resultant aldehyde intermediate to a Wittig reaction to provide α,β-unsaturated esters with only one purification step. The cyclisation of 4-aryl-but-2-enoates is carried out in the presence of stoichiometric amounts of SnCl2∙2H2O and thus this one-pot strategy also permitted the expeditious synthesis of indolines in good yield.
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