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Obituary
Zenichi Yoshida (1925-2023)
Zenichi Yoshida (1925-2023)
Professor. Zenichi Yoshida,
a member of the Honorary Advisors of HETEROCYCLES (1975-1998),
has passed away on May 4, 2023 at the age of 97.
I deeply express my regret over his death.
Kunio Ogasawara
Editor
May 11, 2023
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Communication | Special issue | Vol 90, No. 2, 2015, pp.827-831
Published online, 27th August, 2014
Published online, 27th August, 2014
DOI: 10.3987/COM-14-S(K)58
■ Removal of Xylylene Groups from Tetrakis(o-xylylenedithio)phthalocyanines with Toluene/Aluminum Chloride and Construction of Dithiaphosphole Rings
Takeshi Kimura* and Shiduko Nakajo
*Center for Instrumental Analysis, Iwate University, 4-3-5 Ueda, Morioka, Iwate 020-8551, Japan
Abstract
Xylylene groups were removed from tetrakis(o-xylylenedithio)phthalocyanines via C-S bond cleavage by treatment with toluene and aluminum chloride. Octathiolate anions generated were reacted with dichlorophenylphosphine to produce phthalocyanines with four dithiaphosphole rings. The structures of the products were determined by NMR and FABMS. Electrochemical and optical properties of them were verified by cyclic voltammetry and UV-vis spectroscopy.
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