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Short Paper | Special issue | Vol 95, No. 2, 2017, pp.1230-1244
Published online, 18th November, 2016
DOI: 10.3987/COM-16-S(S)74
Synthesis of a Functionalized Morphan Scaffold via a Palladium-Catalyzed Cycloalkenylation and Beckmann Rearrangement

Natsuko Kagawa, Yutaka Yamamoto, Shuichiro Ono, and Masahiro Toyota*

*Department of Chemistry, Graduate School of Science, Osaka Prefecture University, 1-1 Gakuencho, Sakai, Osaka 599-8531, Japan

Abstract

Functionalized 2-azabicyclo[3.3.1]nonan-3-ones, potential precursors to morphan, were assembled using a combination of a palladium-catalyzed cycloalkenylation and a Beckmann rearrangement.