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Short Paper | Regular issue | Vol 102, No. 2, 2021, pp.318-324
Published online, 18th December, 2020
DOI: 10.3987/COM-20-14360
Synthesis of α-Bromomethyl Ketones in CuBr - bpy System

Abulipizi Gulizhabaier, Hasimujiang Balat, and Abulikemu Abudu Rexit*

*Xinjiang Key Laboratory of Energy Storage and Photoelectrocatalytic Materials and Department of Chemistry, Xinjiang Normal University, Urumqi, China

Abstract

Herein we reported a convenient, regiospecific, efficient and fairly general method for the preparation of α-bromomethyl ketones from α,α,α-tribromomethyl carbinols with 2.2 equivalents of copper(I) bromide and 2,2'-bipyridine in refluxing 1,2-dichloroethane.